Acid-Base Extraction: Separation Of An Organic Aci

Experiment Title: Acid-Base extraction: Separation of an Organic Acid, a Base and a Neutral Compound 1) -Mass of benzoic stifling set-apart = 0.893 g -Percent recovery of benzoic acid = 89.3% -Melting phase of benzoic acid = 121 °C 122 °C -Mass of 4-chloroaniline isolated = 1.2 g -Percent recovery of 4-chloroaniline = 120% -Melting point of 4-chloroaniline = 53°C 60 °C -Mass of naphthalene isolated = 1.36 g -Percent recovery of naphthalene = 136% -Melting point of naphthalene = 65 °C 70 °C 2)The differences in the masses of the compounds onward and after(prenominal) the taste may include the incident that the solids were not dry proscribed completely since the masses afterward were larger than 1 g for both 4-chloroaniline and naphthalene. The wet solids may have added more than weight. ane reason to explain a mass little than 1 g fro Benzoic acid may charter with the possibility that not all of the components of the solid was collected prope rly. in that location may have also been a problem with the modality that the solids were weighed on the scale and this could account for the differences. 3)The reason for the fact that the resolving power employ in an extraction should have a start stewing point is so that the solvent itself can fly out of the mixture.

This allows for theextraction or the drawing out of the compounds so that they could be studied more effectively. 4)The extraction process would be more difficult as the higher icyity of the solvent would pretend little immiscibility with water because water is also a polar tenderness and so there would not be a behave and defined separation of the solve nts. This makes it difficult to drain of the! perforate aqueous layer and to continue with the extractions. Also, the solvent dimethylformamide would dribble prolonged to evaporate due to its higher boiling point and would take a long time to continue with the experiment. 5)The extraction that we did during the experiment is called Acid-Base Extraction because it...If you want to get a full essay, suppose it on our website: OrderEssay.net

If you want to get a full information about our service, visit our page: write my essay